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(2002), Introducing the concept of uncertainty of measurement in testing in association with the application of the standard ISO/IEC 17025, Accred Qual Assur, 7, 79 80 55 International Organization on Harmonization (1995), Guideline for industry: Text on validation of analytical procedures, ICH-Q2A, available: http://wwwfdagov/cder/guidance/indexhtm 56 Huber, L (1998), Validation of analytical methods Part 9, in Huber, L, Ed, Validation and Quali cation in Analytical Laboratories, Interpharm Press, Agilent Technologies, available: http://wwwlabcompliancecom 57 Wells, R J (1998), Validation requirements for chemical methods in quantitative analysis Horses for courses Accred Qual Assur, 3, 189 193 58 Green, M (1996), A practical guide to analytical method validation, Anal Chem, 68, 305A 309A 59 Eurachem Guide (2000), Selection, Use and Interpretation of Pro ciency Testing (PT) Schemes by Laboratories, available: http://wwweurachemorg 60 Eurachem/Eurolab/EA Guide EA-03/04 (2001, Aug.

), Use of Pro ciency Testing as a Tool for Accreditation in Testing, available: http://wwweurachemorg 61 European Committee for Normalisation (CEN), (2006), Standardization and related activities General Vocabulary (from ISO/IEC Guide 2:2004), EN45020:2006, www cenormbe 62 Association of Of cial Analytical Chemists (AOAC) International (2000), Method validation programs (OMA/PVM Department), including Appendix D: Guidelines for collaborative study procedures to validate characteristics of a method of analysis, available: http://wwwaoacorg/vmeth/devmethnohtm 63 Horwitz, W (1995), Protocol for the design, conduct and interpretation of method performance studies, Pure Appl Chem, 67, 331 343 64 Thompson, M, and Wood, R (1993), The international harmonized protocol for the pro ciency testing of (chemical) analytical laboratories, Pure Appl Chem, 65, 2123 2144: also J AOAC Int, 76, 26 940 (1993) 65 Currie, L A.

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(1995), Nomenclature in evaluation of analytical methods including detection and quanti cation capabilities, Pure Appl Chem, 67, 1699 1723 66 Currie, L A, and Svehla, G (1994), Nomenclature for the presentation of results of chemical analysis, International Union of Pure and Applied Chemistry (IUPAC), Pure Appl Chem, 66, 595 608 67 Pocklington, W D (1990), Harmonized protocols for the adoption of standardized analytical methods and for the presentation of their performance characteristics,.

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1. Continue with ab20-01.dwg from the previous exercise. In the dbConnect window, right-click PART NO and choose Edit Table to open the Data Table window. 2. Choose dbConnect Templates New Link Template. 3. Select the PART_NO table and click Continue.

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where r = 0, 1, . . . , n 2, n 1. Consider the sum of (9.P.3) over j = 0, 1, . . . , n. Use this sum to show that

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Flguro 5.4. Location of eigenvolues for two-dimensional linear oscillations. (a) Both modes stable. (b) One mode stable, one mode unstable. (c) Both modes unstable in absence of coupling. (d) Instability induced by coupling. From Courant and Snyder (see Bibliography) with permission.

143 ADVANTAGES OF PSI Traditionally, interferograms have been analyzed by noting the straightness of the fringes or by identifying the fringe centers and assigning a constant surface height along each fringe Adjacent fringes represent a height change of a half wave Finding the fringe centers has been the inherent limit to the precision of the technique and has also restricted the amount of data processing that can be done with the results Visually, the location of the fringe centers can be identi ed to within a tenth or a twentieth of a fringe spacing It is dif cult to precisely locate the maxima or minima of the fringe intensity pattern With a digitized interferogram produced by electronic camera or an input scanner, the situation can be improved to about a ftieth of a wave under ideal situations.

Figure 5.11. (a) A comparison of horizontal line-outs of the far- eld pro les of the lowenergy input pulse (solid line) and the ampli ed output pulse (dashed line). The divergence is unchanged to within the uncertainty of the experimental measurement. (b) Transmission of a 0.5-mm aperture placed at the focus of a 120-cm focal length lens. The expected transmission of this bucket for a 1.25 diffraction-limited beam was calculated to be 96%. A transmission of *92% was measured across the range of output energies up to 25 J.

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